PolyHIPE materials from divinylbenzene were synthesised in the presence of porogens of different chemical structures. These materials possess two levels of porosity: large pores ( 1 20 m) which guarantee the flow of fluids under the application of small pressures and a fine porosity (1 100 nm) present in the walls of the foams which confer to the materials high surface areas (up to 700 m(^2)g(^ 1)). The chemical nature of the porogens employed has a significant influence on the morphologies of the foams affecting both the dimension of the cavities and the fine porous structure. The data collected from both quantitative and qualitative sources were considered within a framework that Identifies distinct patterns of behaviour
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